Information card for entry 7013324

Structure parameters

• Formula: C144 H124 Br8 Cl8 Hg4 O17 P4
• Calculated formula: C144 H124 Br8 Cl8 Hg4 O17 P4
• Title of publication: Tetraphosphinitoresorcinarene complexes: a new structural form for diphosphine mercury(ii) halide complexes
• Authors of publication: Eisler, Dana J.; Puddephatt, Richard J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3567
• a: 41.3843 ± 0.0003 Å
• b: 14.4061 ± 0.0001 Å
• c: 28.1428 ± 0.0002 Å
• α: 90°
• β: 108.864 ± 0.001°
• γ: 90°
• Cell volume: 15877.2 ± 0.2 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0866
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for significantly intense reflections: 0.1409
• Weighted residual factors for all reflections included in the refinement: 0.152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No