Information card for entry 7013325

Structure parameters

• Formula: C152 H164 Cl24 Hg4 O12 P4
• Calculated formula: C152 H164 Cl24 Hg4 O12 P4
• Title of publication: Tetraphosphinitoresorcinarene complexes: a new structural form for diphosphine mercury(ii) halide complexes
• Authors of publication: Eisler, Dana J.; Puddephatt, Richard J.
• Journal of publication: Dalton Transactions
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 3567
• a: 26.6994 ± 0.0002 Å
• b: 16.0482 ± 0.0001 Å
• c: 38.9034 ± 0.0002 Å
• α: 90°
• β: 104.395 ± 0.001°
• γ: 90°
• Cell volume: 16145.9 ± 0.19 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1045
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.0962
• Weighted residual factors for all reflections included in the refinement: 0.1113
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No