Information card for entry 7017741

Structure parameters

• Formula: C90 H144 Cl14 Dy8 N4 O13
• Calculated formula: C90 H144 Cl14 Dy8 N4 O13
• SMILES: CC1=C2C(C)=[N](c3c(cccc3C(C)C)C(C)C)[Dy]34([O]56[Dy](N1c1c(cccc1C(C)C)C(C)C)([O]23)([O]1CCCC1)([Cl][Dy]1235([O]57[Dy]896([O]6CCCC6)([Cl]4)[Cl][Dy]47([O]67[Dy]%10([N](=C(C%11=C(C)N(c%12c(cccc%12C(C)C)C(C)C)[Dy]6([O]%10%11)([O]6CCCC6)([Cl][Dy]57([Cl]1)([O]1CCCC1)([Cl]2)[Cl]9)Cl)C)c1c(cccc1C(C)C)C(C)C)([O]1CCCC1)(Cl)[Cl]4)([O]1CCCC1)([Cl]8)[Cl]3)[O]1CCCC1)Cl)([O]1CCCC1)Cl
• Title of publication: Oxidation and coupling of β-diketiminate ligand in lanthanide complexes: novel eight-nuclear lanthanide clusters with μ-, μ3-Cl, and μ4-O bridge.
• Authors of publication: Zhang, Jie; Zhang, Zhengxing; Chen, Zhenxia; Zhou, Xigeng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 2
• Pages of publication: 357 - 359
• a: 28.668 ± 0.006 Å
• b: 31.282 ± 0.006 Å
• c: 16.199 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14527 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 41
• Hermann-Mauguin space group symbol: A b a 2
• Hall space group symbol: A 2 -2ab
• Residual factor for all reflections: 0.08
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1078
• Weighted residual factors for all reflections included in the refinement: 0.1174
• Goodness-of-fit parameter for all reflections included in the refinement: 0.905
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No