Information card for entry 7017742

Structure parameters

• Formula: C61 H89 N4
• Calculated formula: C61 H89 N4
• Title of publication: Oxidation and coupling of β-diketiminate ligand in lanthanide complexes: novel eight-nuclear lanthanide clusters with μ-, μ3-Cl, and μ4-O bridge.
• Authors of publication: Zhang, Jie; Zhang, Zhengxing; Chen, Zhenxia; Zhou, Xigeng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 2
• Pages of publication: 357 - 359
• a: 12.937 ± 0.004 Å
• b: 13.424 ± 0.004 Å
• c: 17.464 ± 0.006 Å
• α: 86.122 ± 0.005°
• β: 75.906 ± 0.005°
• γ: 71.96 ± 0.005°
• Cell volume: 2796.9 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1323
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.1372
• Weighted residual factors for all reflections included in the refinement: 0.1605
• Goodness-of-fit parameter for all reflections included in the refinement: 0.819
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No