Information card for entry 7018839

Structure parameters

• Formula: C3 H22 Ge K8 Mn N0 O47 W9
• Calculated formula: C3 Ge K8 Mn O47 W9
• Title of publication: Two novel trivacant Keggin-type polytungstates supported manganese carbonyl derivatives synthesized by degradation of metastable [γ-XW10O36]8− (X = GeIV, SiIV)
• Authors of publication: Zhao, Juan; Wang, Junsheng; Zhao, Junwei; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton Transactions
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 19
• Pages of publication: 5832
• a: 12.3018 ± 0.0006 Å
• b: 14.6505 ± 0.0007 Å
• c: 16.4725 ± 0.0008 Å
• α: 71.541 ± 0.001°
• β: 76.22 ± 0.001°
• γ: 81.591 ± 0.001°
• Cell volume: 2726.9 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0526
• Residual factor for significantly intense reflections: 0.0468
• Weighted residual factors for significantly intense reflections: 0.1249
• Weighted residual factors for all reflections included in the refinement: 0.1299
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No