Information card for entry 7018840

Structure parameters

• Formula: C3 H24 K8 Mn N0 O48 Si W9
• Calculated formula: C3 K8 Mn O48 Si W9
• Title of publication: Two novel trivacant Keggin-type polytungstates supported manganese carbonyl derivatives synthesized by degradation of metastable [γ-XW10O36]8− (X = GeIV, SiIV)
• Authors of publication: Zhao, Juan; Wang, Junsheng; Zhao, Junwei; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton Transactions
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 19
• Pages of publication: 5832
• a: 12.265 ± 0.002 Å
• b: 14.692 ± 0.003 Å
• c: 16.497 ± 0.003 Å
• α: 71.58 ± 0.003°
• β: 76.382 ± 0.003°
• γ: 81.643 ± 0.004°
• Cell volume: 2733 ± 0.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0726
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1376
• Weighted residual factors for all reflections included in the refinement: 0.1445
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No