Information card for entry 7018983

Structure parameters

• Formula: C149 H113 N17 O24 Zn10
• Calculated formula: C149 H113 N17 O24 Zn10
• Title of publication: Isolation and characterization of unusual multinuclear Schiff base complexes: rearrangements reactions and octanuclear cluster formation.
• Authors of publication: Martínez Belmonte, Marta; Escudero-Adán, Eduardo C; Martin, Eddy; Kleij, Arjan W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 17
• Pages of publication: 5193 - 5200
• a: 12.9382 ± 0.0011 Å
• b: 13.9784 ± 0.0013 Å
• c: 18.3443 ± 0.0016 Å
• α: 83.265 ± 0.003°
• β: 87.458 ± 0.003°
• γ: 88.388 ± 0.003°
• Cell volume: 3290.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1009
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No