Information card for entry 7018984

Structure parameters

• Formula: C61.7 H62 N4 O16.38 S1.02 Zn4
• Calculated formula: C61.7 H62 N4 O16.375 S1.025 Zn4
• Title of publication: Isolation and characterization of unusual multinuclear Schiff base complexes: rearrangements reactions and octanuclear cluster formation.
• Authors of publication: Martínez Belmonte, Marta; Escudero-Adán, Eduardo C; Martin, Eddy; Kleij, Arjan W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 17
• Pages of publication: 5193 - 5200
• a: 17.7411 ± 0.0012 Å
• b: 18.4397 ± 0.0013 Å
• c: 24.5458 ± 0.0016 Å
• α: 88.7 ± 0.002°
• β: 75.454 ± 0.002°
• γ: 62.681 ± 0.002°
• Cell volume: 6865.5 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.119
• Residual factor for significantly intense reflections: 0.0705
• Weighted residual factors for significantly intense reflections: 0.2035
• Weighted residual factors for all reflections included in the refinement: 0.243
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No