Information card for entry 7019369

Structure parameters

• Formula: C12 H120 K2 N2 Nd4 O136 Si2 W22
• Calculated formula: C12 H10 K2 N2 Nd4 O136 Si2 W22
• Title of publication: A series of three-dimensional architectures constructed from lanthanide-substituted polyoxometalosilicates and lanthanide cations or lanthanide-organic complexes as linkers.
• Authors of publication: An, Haiyan; Zhang, Hua; Chen, Zhaofei; Li, Yangguang; Liu, Xuan; Chen, Hao
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 27
• Pages of publication: 8390 - 8400
• a: 18.6271 ± 0.0012 Å
• b: 17.6188 ± 0.0011 Å
• c: 22.2471 ± 0.0011 Å
• α: 90°
• β: 121.492 ± 0.004°
• γ: 90°
• Cell volume: 6225.8 ± 0.7 ų
• Cell temperature: 185 K
• Ambient diffraction temperature: 185 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.0312
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0769
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No