Information card for entry 7019385

Structure parameters

• Formula: C18 H24 N4 Ni O24 S2 Yb2
• Calculated formula: C18 H24 N4 Ni O24 S2 Yb2
• Title of publication: Hydrothermal synthesis, crystal structure and properties of Ni(ii)-4f complexes based on 1H-benzimidazole-5,6-dicarboxylic acid.
• Authors of publication: Sun, Ya-Guang; Xiong, Gang; Guo, Mei-Yan; Ding, Fu; Wang, Shu-Ju; Smet, Philippe F.; Poelman, Dirk; Gao, En-Jun; Verpoort, Francis
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 25
• Pages of publication: 7670 - 7680
• a: 15.408 ± 0.003 Å
• b: 8.5449 ± 0.0013 Å
• c: 24.386 ± 0.004 Å
• α: 90°
• β: 115.573 ± 0.009°
• γ: 90°
• Cell volume: 2896.1 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0294
• Residual factor for significantly intense reflections: 0.0289
• Weighted residual factors for significantly intense reflections: 0.0732
• Weighted residual factors for all reflections included in the refinement: 0.0737
• Goodness-of-fit parameter for all reflections included in the refinement: 1.183
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No