Information card for entry 7019924

Structure parameters

• Common name: (Ar(tBuCH2)N)2(tBuC(H)NAr)TaP(H)Ph
• Formula: C48.75 H73 N3 P Ta
• Calculated formula: C48.75 H73 N3 P Ta
• Title of publication: Terminal phosphinidene formation via tantalaziridine complexes.
• Authors of publication: Rankin, Matthew A.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 32
• Pages of publication: 9615 - 9618
• a: 12.8823 ± 0.0008 Å
• b: 17.7431 ± 0.0012 Å
• c: 21.9477 ± 0.0015 Å
• α: 84.424 ± 0.001°
• β: 74.16 ± 0.001°
• γ: 87.807 ± 0.001°
• Cell volume: 4802.9 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0643
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0814
• Weighted residual factors for all reflections included in the refinement: 0.092
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No