Information card for entry 7019925

Structure parameters

• Common name: (Ar(tBuCH2)N)3TaPCy
• Formula: C45 H71 N3 P Ta
• Calculated formula: C45 H71 N3 P Ta
• Title of publication: Terminal phosphinidene formation via tantalaziridine complexes.
• Authors of publication: Rankin, Matthew A.; Cummins, Christopher C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 32
• Pages of publication: 9615 - 9618
• a: 10.932 ± 0.0012 Å
• b: 11.5291 ± 0.0012 Å
• c: 18.468 ± 0.002 Å
• α: 102.234 ± 0.002°
• β: 91.533 ± 0.002°
• γ: 103.933 ± 0.002°
• Cell volume: 2200.4 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0432
• Residual factor for significantly intense reflections: 0.0329
• Weighted residual factors for significantly intense reflections: 0.0655
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No