Crystallography Open Database

Information card for entry 7020521

7020520 << 7020521 >> 7020522

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Coordinates	7020521.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66.5 H69 P5 Pd2 Si
Calculated formula	C66.5 H69 P5 Pd2 Si
Title of publication	Coordination chemistry of trimethylsilylphosphaalkyne: a phosphaalkyne bearing a reactive substituent.
Authors of publication	Mansell, Stephen M.; Green, Michael; Russell, Christopher A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	47
Pages of publication	14360 - 14368
a	11.1118 ± 0.0002 Å
b	14.1587 ± 0.0003 Å
c	20.7997 ± 0.0005 Å
α	79.438 ± 0.001°
β	83.553 ± 0.001°
γ	67.897 ± 0.001°
Cell volume	2977.16 ± 0.11 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1269
Residual factor for significantly intense reflections	0.0744
Weighted residual factors for significantly intense reflections	0.1284
Weighted residual factors for all reflections included in the refinement	0.1508
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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