Information card for entry 7020522

Structure parameters

• Formula: C116 H118 P8 Pd5 Si3
• Calculated formula: C116 H118 P8 Pd5 Si3
• Title of publication: Coordination chemistry of trimethylsilylphosphaalkyne: a phosphaalkyne bearing a reactive substituent.
• Authors of publication: Mansell, Stephen M.; Green, Michael; Russell, Christopher A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 47
• Pages of publication: 14360 - 14368
• a: 14.936 ± 0.002 Å
• b: 15 ± 0.002 Å
• c: 27.47 ± 0.004 Å
• α: 87.751 ± 0.008°
• β: 80.249 ± 0.007°
• γ: 71.765 ± 0.007°
• Cell volume: 5760.2 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for significantly intense reflections: 0.1527
• Weighted residual factors for all reflections included in the refinement: 0.1733
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No