Information card for entry 7021007

Structure parameters

• Formula: C70.85 H156.4 Cl4 Cu4 Ge6 N12 Si6
• Calculated formula: C70.85 H156.4 Cl4 Cu4 Ge6 N12 Si6
• Title of publication: Heavier carbene analogues and their derivatives as κ-El, κ(2)-El,N, and κ(2)-N,N' ligands: different reactivity patterns for acyclic and cyclic diamidogermylenes and -stannylenes.
• Authors of publication: West, Joseph K.; Fondong, Gregory L.; Noll, Bruce C.; Stahl, Lothar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 11
• Pages of publication: 3835 - 3842
• a: 12.6839 ± 0.0014 Å
• b: 15.6668 ± 0.0017 Å
• c: 16.3267 ± 0.0017 Å
• α: 101.88 ± 0.0017°
• β: 111.442 ± 0.0016°
• γ: 108.31 ± 0.0016°
• Cell volume: 2671.5 ± 0.5 ų
• Cell temperature: 173.15 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0454
• Residual factor for significantly intense reflections: 0.0371
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.1122
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No