Information card for entry 7021375

Structure parameters

• Formula: C75 H84 Ge4 N4 O8 Pd
• Calculated formula: C75 H84 Ge4 N4 O8 Pd
• SMILES: [Pd]([Ge]12[N](C)(CCO1)CC(O2)(c1ccccc1)c1ccccc1)([Ge]12[N](C)(CCO1)CC(O2)(c1ccccc1)c1ccccc1)([Ge]12[N](C)(CCO1)CC(O2)(c1ccccc1)c1ccccc1)[Ge]12[N](C)(CCO1)CC(O2)(c1ccccc1)c1ccccc1.c1(ccccc1)C
• Title of publication: Palladium complexes with stabilized germylene and stannylene ligands.
• Authors of publication: Kireenko, Marina M.; Zaitsev, Kirill V.; Oprunenko, Yuri F.; Churakov, Andrei V.; Tafeenko, Viktor A.; Karlov, Sergey S.; Zaitseva, Galina S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 22
• Pages of publication: 7901 - 7912
• a: 15.2818 ± 0.0019 Å
• b: 16.426 ± 0.002 Å
• c: 17.317 ± 0.002 Å
• α: 94.652 ± 0.002°
• β: 115.307 ± 0.002°
• γ: 113.764 ± 0.002°
• Cell volume: 3423.8 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0503
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No