Information card for entry 7021376

Structure parameters

• Formula: C52 H58 N2 O4 Pd
• Calculated formula: C52 H58 N2 O4 Pd
• Title of publication: Palladium complexes with stabilized germylene and stannylene ligands.
• Authors of publication: Kireenko, Marina M.; Zaitsev, Kirill V.; Oprunenko, Yuri F.; Churakov, Andrei V.; Tafeenko, Viktor A.; Karlov, Sergey S.; Zaitseva, Galina S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 22
• Pages of publication: 7901 - 7912
• a: 29.222 ± 0.004 Å
• b: 11.0428 ± 0.0014 Å
• c: 14.8017 ± 0.0019 Å
• α: 90°
• β: 110.719 ± 0.002°
• γ: 90°
• Cell volume: 4467.5 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0321
• Weighted residual factors for significantly intense reflections: 0.0921
• Weighted residual factors for all reflections included in the refinement: 0.0976
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No