Information card for entry 7021647

Structure parameters

• Common name: (dihydrido-tetrakis(trimethylphosphine)-cobalt(iii))(tris-bis- 3,5-(trifluorometh
• Chemical name: [dihydrido-tetrakis(trimethylphosphine)-cobalt(iii)][tris-bis-3,5-(trifluoromethyl)pyrazolate-trimethylphosphine-cobalt(ii)]
• Formula: C30 H50 Co2 F18 N6 P5
• Calculated formula: C30 H50 Co2 F18 N6 P5
• Title of publication: Synthesis and structures of Co bis-trifluoromethylpyrazolate complexes.
• Authors of publication: Rivers, Joseph H.; Jones, Richard A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 12898 - 12907
• a: 10.0753 ± 0.0002 Å
• b: 68.7275 ± 0.0012 Å
• c: 13.723 ± 0.0009 Å
• α: 90°
• β: 90.308 ± 0.006°
• γ: 90°
• Cell volume: 9502.4 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1697
• Residual factor for significantly intense reflections: 0.1018
• Weighted residual factors for significantly intense reflections: 0.129
• Weighted residual factors for all reflections included in the refinement: 0.1443
• Goodness-of-fit parameter for all reflections included in the refinement: 1.294
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No