Information card for entry 7022244

Structure parameters

• Formula: C6 H24 In2 N6 Ni S7 Sb2
• Calculated formula: C6 H24 In2 N6 Ni S7 Sb2
• Title of publication: Solvothermal synthesis and characterization of thioindate-thioantimonates with transition-metal complexes: the first examples of the incorporation of transition metal ions into In-S-Sb frameworks.
• Authors of publication: Zhou, Jian; Liu, Xing; An, Litao; Hu, Feilong; Kan, Yuhe; Li, Rong; Shen, Zhenming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 5
• Pages of publication: 1735 - 1742
• a: 11.2605 ± 0.0011 Å
• b: 17.1278 ± 0.0016 Å
• c: 13.6829 ± 0.001 Å
• α: 90°
• β: 117.255 ± 0.006°
• γ: 90°
• Cell volume: 2346 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0955
• Residual factor for significantly intense reflections: 0.0855
• Weighted residual factors for significantly intense reflections: 0.1924
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No