Information card for entry 7022245

Structure parameters

• Formula: C20 H80 In6 N20 Ni3 S21 Sb6
• Calculated formula: C20 H80 In6 N20 Ni3 S21 Sb6
• Title of publication: Solvothermal synthesis and characterization of thioindate-thioantimonates with transition-metal complexes: the first examples of the incorporation of transition metal ions into In-S-Sb frameworks.
• Authors of publication: Zhou, Jian; Liu, Xing; An, Litao; Hu, Feilong; Kan, Yuhe; Li, Rong; Shen, Zhenming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 5
• Pages of publication: 1735 - 1742
• a: 25.819 ± 0.005 Å
• b: 11.161 ± 0.002 Å
• c: 30.147 ± 0.006 Å
• α: 90°
• β: 110.42 ± 0.03°
• γ: 90°
• Cell volume: 8141 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0924
• Weighted residual factors for all reflections included in the refinement: 0.0965
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No