Crystallography Open Database

Information card for entry 7022712

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Coordinates	7022712.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C76 H126 N12 O7 Y2
Calculated formula	C76 H86 N12 O7 Y2
Title of publication	Unprecedented reaction of bridged bis(guanidinate) lanthanide complexes: sterically induced deprotonation.
Authors of publication	Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Zhang, Yong; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	19
Pages of publication	7009 - 7018
a	27.2799 ± 0.0011 Å
b	18.1316 ± 0.0007 Å
c	16.7684 ± 0.0007 Å
α	90°
β	105.244 ± 0.004°
γ	90°
Cell volume	8002.3 ± 0.6 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0732
Residual factor for significantly intense reflections	0.0492
Weighted residual factors for significantly intense reflections	0.1279
Weighted residual factors for all reflections included in the refinement	0.1374
Goodness-of-fit parameter for all reflections included in the refinement	1.04
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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