Information card for entry 7022713

Structure parameters

• Formula: C81 H106 Cl2 N14 Yb2
• Calculated formula: C81 H98 Cl2 N14 Yb2
• Title of publication: Unprecedented reaction of bridged bis(guanidinate) lanthanide complexes: sterically induced deprotonation.
• Authors of publication: Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Zhang, Yong; Shen, Qi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 19
• Pages of publication: 7009 - 7018
• a: 11.4364 ± 0.0018 Å
• b: 12.8922 ± 0.0015 Å
• c: 15.651 ± 0.003 Å
• α: 72.96 ± 0.02°
• β: 84.03 ± 0.03°
• γ: 64.624 ± 0.019°
• Cell volume: 1992.8 ± 0.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1167
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No