Crystallography Open Database

Information card for entry 7022714

Preview

Coordinates	7022714.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H96 N14 O Yb2
Calculated formula	C66 H88 N14 O Yb2
Title of publication	Unprecedented reaction of bridged bis(guanidinate) lanthanide complexes: sterically induced deprotonation.
Authors of publication	Wang, Chuanyong; Zhang, Xingmin; Xue, Mingqiang; Zhang, Yong; Shen, Qi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	19
Pages of publication	7009 - 7018
a	11.5151 ± 0.0006 Å
b	12.9495 ± 0.0008 Å
c	13.0112 ± 0.0007 Å
α	98.036 ± 0.005°
β	92.863 ± 0.004°
γ	116.207 ± 0.006°
Cell volume	1709.95 ± 0.19 Å³
Cell temperature	220 ± 2 K
Ambient diffraction temperature	220 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0521
Residual factor for significantly intense reflections	0.0434
Weighted residual factors for significantly intense reflections	0.1046
Weighted residual factors for all reflections included in the refinement	0.1091
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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