Information card for entry 7023527

Structure parameters

• Formula: C73 H71 Cl6 F20 N3 O P6 Pd2
• Calculated formula: C73 H69 Cl6.005 F20 N3 O P6 Pd2
• Title of publication: Flexible, linear, tetranuclear palladium complexes supported by tetraphosphine ligands with electron-withdrawing groups.
• Authors of publication: Tanase, Tomoaki; Hatada, Satoko; Mochizuki, Ayaka; Nakamae, Kanako; Kure, Bunsho; Nakajima, Takayuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 45
• Pages of publication: 15941 - 15952
• a: 12.688 ± 0.003 Å
• b: 15.676 ± 0.004 Å
• c: 23.273 ± 0.006 Å
• α: 93.852 ± 0.003°
• β: 93.895 ± 0.0018°
• γ: 110.859 ± 0.003°
• Cell volume: 4294.8 ± 1.9 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.2533
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No