Information card for entry 7023528

Structure parameters

• Formula: C99.5 H81 Cl7 F28 N2 P10 Pd2
• Calculated formula: C99.5 H78 Cl7 F28 N2 P10 Pd2
• Title of publication: Flexible, linear, tetranuclear palladium complexes supported by tetraphosphine ligands with electron-withdrawing groups.
• Authors of publication: Tanase, Tomoaki; Hatada, Satoko; Mochizuki, Ayaka; Nakamae, Kanako; Kure, Bunsho; Nakajima, Takayuki
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 45
• Pages of publication: 15941 - 15952
• a: 22.575 ± 0.0005 Å
• b: 16.5211 ± 0.0004 Å
• c: 29.1443 ± 0.0007 Å
• α: 90°
• β: 91.3229 ± 0.0012°
• γ: 90°
• Cell volume: 10866.9 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0827
• Weighted residual factors for all reflections included in the refinement: 0.247
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No