Information card for entry 7023984

Structure parameters

• Formula: C16 H31 Bi N2 O3 Si2
• Calculated formula: C16 H31 Bi N2 O3 Si2
• SMILES: [Bi]123(O[Si](C)(C)O[Si](O1)(C)C)[N](Cc1c2c(C[N]3(C)C)ccc1)(C)C
• Title of publication: Straightforward synthesis of novel cyclic metallasiloxanes supported by an N,C,N-chelating ligand.
• Authors of publication: Fridrichová, Adéla; Mairychová, Barbora; Padělková, Zdeňka; Lyčka, Antonín; Jurkschat, Klaus; Jambor, Roman; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 46
• Pages of publication: 16403 - 16411
• a: 13.178 ± 0.0012 Å
• b: 11.192 ± 0.001 Å
• c: 15.8121 ± 0.0019 Å
• α: 90°
• β: 105.551 ± 0.006°
• γ: 90°
• Cell volume: 2246.7 ± 0.4 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1039
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.13
• Weighted residual factors for all reflections included in the refinement: 0.1588
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No