Information card for entry 7023985

Structure parameters

• Formula: C48 H58 N4 O4 Sb2 Si2
• Calculated formula: C48 H58 N4 O4 Sb2 Si2
• SMILES: c1(ccccc1)[Si]1(O[Sb](c2c(cccc2CN(C)C)CN(C)C)O[Si](O[Sb](c2c(cccc2CN(C)C)CN(C)C)O1)(c1ccccc1)c1ccccc1)c1ccccc1
• Title of publication: Straightforward synthesis of novel cyclic metallasiloxanes supported by an N,C,N-chelating ligand.
• Authors of publication: Fridrichová, Adéla; Mairychová, Barbora; Padělková, Zdeňka; Lyčka, Antonín; Jurkschat, Klaus; Jambor, Roman; Dostál, Libor
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 46
• Pages of publication: 16403 - 16411
• a: 11.708 ± 0.0005 Å
• b: 15.9991 ± 0.001 Å
• c: 13.749 ± 0.0006 Å
• α: 90°
• β: 113.078 ± 0.004°
• γ: 90°
• Cell volume: 2369.3 ± 0.2 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0437
• Residual factor for significantly intense reflections: 0.0291
• Weighted residual factors for significantly intense reflections: 0.0592
• Weighted residual factors for all reflections included in the refinement: 0.0662
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No