Information card for entry 7026988

Structure parameters

• Formula: C57 H71 Cl2 F6 N10 O14 P Ru
• Calculated formula: C57 H59 Cl1.7 F6 N10 O12.8 P Ru
• Title of publication: Stepwise synthetic strategy for the preparation of trinuclear complexes of bis(terpyridyl) bridging ligands containing aza-crown macrocyclic spacer groups
• Authors of publication: Bushell, Karen L.; Couchman, Samantha M.; Jeffery, John C.; Rees, Leigh H.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 20
• Pages of publication: 3397
• a: 8.357 ± 0.004 Å
• b: 17.697 ± 0.005 Å
• c: 22.442 ± 0.008 Å
• α: 76.16 ± 0.03°
• β: 87.85 ± 0.02°
• γ: 81.87 ± 0.02°
• Cell volume: 3190 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1476
• Residual factor for significantly intense reflections: 0.1044
• Weighted residual factors for significantly intense reflections: 0.282
• Weighted residual factors for all reflections included in the refinement: 0.3185
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No