Information card for entry 7026989

Structure parameters

• Formula: C74.22 H77.6 F16.17 N12 O5.81 P2.7 Ru
• Calculated formula: C74.256 H67 F16.116 N12 O5.814 P2.686 Ru
• Title of publication: Stepwise synthetic strategy for the preparation of trinuclear complexes of bis(terpyridyl) bridging ligands containing aza-crown macrocyclic spacer groups
• Authors of publication: Bushell, Karen L.; Couchman, Samantha M.; Jeffery, John C.; Rees, Leigh H.; Ward, Michael D.
• Journal of publication: Journal of the Chemical Society, Dalton Transactions
• Year of publication: 1998
• Journal issue: 20
• Pages of publication: 3397
• a: 11.417 ± 0.004 Å
• b: 18.318 ± 0.009 Å
• c: 20.444 ± 0.009 Å
• α: 76.4 ± 0.03°
• β: 88.87 ± 0.05°
• γ: 81.32 ± 0.04°
• Cell volume: 4108 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.239
• Residual factor for significantly intense reflections: 0.1329
• Weighted residual factors for significantly intense reflections: 0.3461
• Weighted residual factors for all reflections included in the refinement: 0.429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No