Information card for entry 7028660

Structure parameters

• Common name: [(EtOH)DiPPIm]2AgBF4
• Formula: C38 H58 Ag B F4 N4 O3
• Calculated formula: C38 H58 Ag B F4 N4 O3
• Title of publication: Synthesis and characterization of oxygen-functionalised-NHC silver(i) complexes and NHC transmetallation to nickel(ii).
• Authors of publication: Hameury, Sophie; de Frémont, Pierre; R Breuil, Pierre-Alain; Olivier-Bourbigou, Hélène; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 12
• Pages of publication: 4700 - 4710
• a: 12.1561 ± 0.0005 Å
• b: 13.6336 ± 0.0006 Å
• c: 14.9663 ± 0.0006 Å
• α: 84.3002 ± 0.0019°
• β: 66.395 ± 0.002°
• γ: 66.881 ± 0.002°
• Cell volume: 2085.38 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1064
• Residual factor for significantly intense reflections: 0.0678
• Weighted residual factors for significantly intense reflections: 0.1553
• Weighted residual factors for all reflections included in the refinement: 0.1706
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No