Information card for entry 7028661

Structure parameters

• Common name: [(EtOMe)DiPPIm]2AgCl
• Formula: C36 H54 Ag Cl N4 O3
• Calculated formula: C36 H54 Ag Cl N4 O3
• Title of publication: Synthesis and characterization of oxygen-functionalised-NHC silver(i) complexes and NHC transmetallation to nickel(ii).
• Authors of publication: Hameury, Sophie; de Frémont, Pierre; R Breuil, Pierre-Alain; Olivier-Bourbigou, Hélène; Braunstein, Pierre
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 12
• Pages of publication: 4700 - 4710
• a: 8.8012 ± 0.0003 Å
• b: 11.5154 ± 0.0005 Å
• c: 19.3453 ± 0.0012 Å
• α: 97.641 ± 0.002°
• β: 102.77 ± 0.003°
• γ: 92.692 ± 0.003°
• Cell volume: 1889.24 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0788
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.1059
• Weighted residual factors for all reflections included in the refinement: 0.1159
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No