Information card for entry 7028987

Structure parameters

• Formula: C67 H46 Co15 N2 O38 Pd9
• Calculated formula: C67.005 H46 Co15.003 N2 O38.005 Pd9.005
• Title of publication: Structural rearrangements induced by acid-base reactions in metal carbonyl clusters: the case of [H3-nCo15Pd9C3(CO)38](n-) (n = 0-3).
• Authors of publication: Ciabatti, Iacopo; Femoni, Cristina; Gaboardi, Mattia; Iapalucci, Maria Carmela; Longoni, Giuliano; Pontiroli, Daniele; Riccò, Mauro; Zacchini, Stefano
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 11
• Pages of publication: 4388 - 4399
• a: 12.8483 ± 0.001 Å
• b: 35.86 ± 0.003 Å
• c: 17.9822 ± 0.0013 Å
• α: 90°
• β: 92.099 ± 0.001°
• γ: 90°
• Cell volume: 8279.6 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1135
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.168
• Weighted residual factors for all reflections included in the refinement: 0.1985
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No