Information card for entry 7029974

Structure parameters

• Formula: C5 H29 Cl2 Cu4 O32 Tb
• Calculated formula: C5 H29 Cl2 Cu4 O32 Tb
• Title of publication: Two one-dimensional compounds based on pyramidal {TbCu4} units and formate ligand: chair-like [(H2O)2(ClO4)2]2- clusters and slow relaxation of magnetization.
• Authors of publication: Li, Zhong-Yi; Yang, Jing-Si; Liu, Rui-Bin; Zhang, Jian-Jun; Liu, Shu-Qin; Ni, Jun; Duan, Chun-Ying
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 43
• Pages of publication: 13264 - 13266
• a: 8.4356 ± 0.0019 Å
• b: 18.837 ± 0.004 Å
• c: 10.116 ± 0.002 Å
• α: 90°
• β: 113.266 ± 0.002°
• γ: 90°
• Cell volume: 1476.7 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0845
• Weighted residual factors for all reflections included in the refinement: 0.0862
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No