Information card for entry 7029975

Structure parameters

• Formula: C4 H30 Cl5 Cu4 Na2 O43 Tb
• Calculated formula: C4 H30 Cl5 Cu4 Na2 O42.66 Tb
• Title of publication: Two one-dimensional compounds based on pyramidal {TbCu4} units and formate ligand: chair-like [(H2O)2(ClO4)2]2- clusters and slow relaxation of magnetization.
• Authors of publication: Li, Zhong-Yi; Yang, Jing-Si; Liu, Rui-Bin; Zhang, Jian-Jun; Liu, Shu-Qin; Ni, Jun; Duan, Chun-Ying
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 43
• Pages of publication: 13264 - 13266
• a: 13.117 ± 0.004 Å
• b: 14.41 ± 0.004 Å
• c: 21.239 ± 0.006 Å
• α: 90°
• β: 102.672 ± 0.004°
• γ: 90°
• Cell volume: 3917 ± 2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0404
• Weighted residual factors for significantly intense reflections: 0.1103
• Weighted residual factors for all reflections included in the refinement: 0.1112
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No