Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
Authors of publication
Armbruster, Felix; Fernández, Ignacio; Breher, Frank
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
29
Pages of publication
5612 - 5626
a
7.972 ± 0.0016 Å
b
13.566 ± 0.003 Å
c
15.596 ± 0.003 Å
α
76.99 ± 0.03°
β
83.98 ± 0.03°
γ
83.97 ± 0.03°
Cell volume
1628.5 ± 0.6 Å3
Cell temperature
200 ± 2 K
Ambient diffraction temperature
200 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1133
Residual factor for significantly intense reflections
0.0624
Weighted residual factors for significantly intense reflections
0.1456
Weighted residual factors for all reflections included in the refinement
0.1736
Goodness-of-fit parameter for all reflections included in the refinement
