Information card for entry 7030639

Structure parameters

• Formula: C20 H28 Cl2 N8 Si2
• Calculated formula: C20 H28 Cl2 N8 Si2
• SMILES: n1(nc(cc1C)C)[Si]12(n3[n](c(cc3C)C)[Si]2(n2nc(cc2C)C)(n2[n]1c(cc2C)C)Cl)Cl
• Title of publication: Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
• Authors of publication: Armbruster, Felix; Fernández, Ignacio; Breher, Frank
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 29
• Pages of publication: 5612 - 5626
• a: 11.486 ± 0.002 Å
• b: 10.342 ± 0.002 Å
• c: 20.67 ± 0.004 Å
• α: 90°
• β: 105.65 ± 0.03°
• γ: 90°
• Cell volume: 2364.3 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0799
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1245
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.12
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7001722
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No