Information card for entry 7030936

Structure parameters

• Formula: C54 H66 N3 P2 Si2 Y
• Calculated formula: C54 H66 N3 P2 Si2 Y
• Title of publication: Differences in the cyclometalation reactivity of bisphosphinimine-supported organo-rare earth complexes.
• Authors of publication: Zamora, Matthew T.; Johnson, Kevin R. D.; Hänninen, Mikko M; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2014
• Journal volume: 43
• Journal issue: 28
• Pages of publication: 10739 - 10750
• a: 9.737 ± 0.0007 Å
• b: 12.1842 ± 0.0009 Å
• c: 24.1371 ± 0.0018 Å
• α: 84.8276 ± 0.0009°
• β: 78.9662 ± 0.0009°
• γ: 69.6098 ± 0.0009°
• Cell volume: 2633.7 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.0999
• Weighted residual factors for all reflections included in the refinement: 0.1031
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No