Information card for entry 7031085

Structure parameters

• Formula: C20 H18 N2 O4.5 V
• Calculated formula: C20 H17.5 N2 O4.5 V
• Title of publication: Biphenyl derived Schiff-base vanadium(V) complexes with pendant OH-groups‒structure, characterization and hydrogen peroxide mediated sulfide oxygenation.
• Authors of publication: Plitt, Patrick; Pritzkow, Hans; Kramer, Roland
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 15
• Pages of publication: 2314 - 2320
• a: 15.3045 ± 0.0007 Å
• b: 8.8087 ± 0.0004 Å
• c: 13.3399 ± 0.0006 Å
• α: 90°
• β: 98.687 ± 0.001°
• γ: 90°
• Cell volume: 1777.76 ± 0.14 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0363
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0865
• Weighted residual factors for all reflections included in the refinement: 0.0912
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No