Information card for entry 7031086

Structure parameters

• Formula: C29 H29 Cl P2 Pd
• Calculated formula: C29 H29 Cl P2 Pd
• Title of publication: [upper bond 1 start]PdCl[PPh(2)CH(2)CH(2)C[upper bond 1 end]HCH(2)CH(2)PPh(2)] as a precursor to homo- and hetero-metallic species directed by ESMS (electrospray ionisation mass spectrometry).
• Authors of publication: Neo, Kian Eang; Neo, Yew Chin; Chien, Sheau Wei; Tan, Geok Kheng; Wilkins, Alistair L.; Henderson, William; Hor, T. S. Andy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2004
• Journal issue: 15
• Pages of publication: 2281 - 2287
• a: 8.56 ± 0.002 Å
• b: 15.276 ± 0.004 Å
• c: 20.019 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2617.7 ± 1.1 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1034
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1339
• Goodness-of-fit parameter for all reflections included in the refinement: 0.962
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No