Information card for entry 7034738

Structure parameters

• Formula: C185 H244 Cl6 N6 O12 Si12 Zr3
• Calculated formula: C185 H244 Cl6 N6 O12 Si12 Zr3
• Title of publication: Group 4 metal compounds incorporating the amide ligand, [N(SiMe2{C6H4-2-OMe})2](.).
• Authors of publication: Evans, Lloyd T. J.; Farnaby, Joy H.; Coles, Martyn P.; Cloke, F Geoffrey N; Hitchcock, Peter B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 19
• Pages of publication: 8950 - 8958
• a: 33.2755 ± 0.0002 Å
• b: 20.1404 ± 0.0001 Å
• c: 28.4984 ± 0.0002 Å
• α: 90°
• β: 97.67°
• γ: 90°
• Cell volume: 18928.2 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0931
• Residual factor for significantly intense reflections: 0.0784
• Weighted residual factors for significantly intense reflections: 0.2077
• Weighted residual factors for all reflections included in the refinement: 0.2177
• Goodness-of-fit parameter for all reflections included in the refinement: 1.194
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No