Information card for entry 7035214

Structure parameters

• Chemical name: PhGe5
• Formula: C70 H50 Ge5
• Calculated formula: C70 H50 Ge5
• Title of publication: Stepwise synthesis and characterization of germa[4], [5], [8], and [10]pericyclynes.
• Authors of publication: Tanimoto, Hiroki; Nagao, Tomohiko; Fujiwara, Taro; Nishiyama, Yasuhiro; Morimoto, Tsumoru; Suzuka, Toshimasa; Tsutsumi, Ken; Kakiuchi, Kiyomi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2015
• Journal volume: 44
• Journal issue: 26
• Pages of publication: 11811 - 11818
• a: 17.5446 ± 0.0003 Å
• b: 25.9092 ± 0.0005 Å
• c: 27.6526 ± 0.0005 Å
• α: 90°
• β: 103.989 ± 0.001°
• γ: 90°
• Cell volume: 12197.1 ± 0.4 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1209
• Residual factor for significantly intense reflections: 0.076
• Weighted residual factors for significantly intense reflections: 0.1746
• Weighted residual factors for all reflections included in the refinement: 0.1948
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No