Information card for entry 7039044

Structure parameters

• Formula: C85 H94 B16 Cl2 N2 P4 Rh2 S2
• Calculated formula: C85 H94 B16 Cl2 N2 P4 Rh2 S2
• Title of publication: Postsynthetic modifications of [2,2,2-(H)(PPh3)2-closo-2,1-RhSB8H8] with Lewis bases: cluster modular tuning.
• Authors of publication: Luaces, Susana; Passarelli, Vincenzo; Artigas, María José; Lahoz, Fernando J.; Oro, Luis A.; Macías, Ramón
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2016
• Journal volume: 45
• Journal issue: 20
• Pages of publication: 8622 - 8636
• a: 11.2617 ± 0.0012 Å
• b: 13.1022 ± 0.0014 Å
• c: 16.6998 ± 0.0018 Å
• α: 79.279 ± 0.001°
• β: 75.554 ± 0.001°
• γ: 65.062 ± 0.001°
• Cell volume: 2154.5 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0396
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No