Information card for entry 7042073

Structure parameters

• Common name: 16232_Complex_1-H
• Formula: C42 H64 Al N4 P3 Rh
• Calculated formula: C42 H64 Al N4 P3 Rh
• Title of publication: Structure and dynamic NMR behavior of rhodium complexes supported by Lewis acidic group 13 metallatranes.
• Authors of publication: Moore, James T.; Smith, Nicholas E.; Lu, Connie C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5689 - 5701
• a: 11.611 ± 0.007 Å
• b: 14.168 ± 0.008 Å
• c: 14.28 ± 0.008 Å
• α: 69.082 ± 0.007°
• β: 77.64 ± 0.007°
• γ: 82.728 ± 0.007°
• Cell volume: 2140 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No