Information card for entry 7042074

Structure parameters

• Common name: 16250_Complex-1-CH3
• Formula: C42.89 H65.68 Al Cl0.11 N4 P3 Rh
• Calculated formula: C42.893 H65.679 Al Cl0.107 N4 P3 Rh
• Title of publication: Structure and dynamic NMR behavior of rhodium complexes supported by Lewis acidic group 13 metallatranes.
• Authors of publication: Moore, James T.; Smith, Nicholas E.; Lu, Connie C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 46
• Journal issue: 17
• Pages of publication: 5689 - 5701
• a: 12.3599 ± 0.0003 Å
• b: 13.5401 ± 0.0003 Å
• c: 14.2951 ± 0.0003 Å
• α: 67.2469 ± 0.0011°
• β: 81.64 ± 0.0011°
• γ: 76.0822 ± 0.0012°
• Cell volume: 2137.74 ± 0.09 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.1134
• Weighted residual factors for all reflections included in the refinement: 0.1168
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No