Information card for entry 7043881

Structure parameters

• Formula: C19.5 H21 Cl N10 Ni
• Calculated formula: C19.5 H21 Cl N10 Ni
• Title of publication: Heteroleptic nickel(II)-diNHC complexes and unusual ‘reverse’ carbene-transfer to silver(I)
• Authors of publication: Huynh, Han Vinh; Koh, Christine Hui Min; Nguyen, Van Ha
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 8.1139 ± 0.0009 Å
• b: 11.2775 ± 0.0013 Å
• c: 12.7151 ± 0.0014 Å
• α: 93.185 ± 0.003°
• β: 104.866 ± 0.003°
• γ: 107.323 ± 0.002°
• Cell volume: 1062.5 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.094
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.1434
• Weighted residual factors for all reflections included in the refinement: 0.1715
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No