Information card for entry 7043882

Structure parameters

• Formula: C23 H25 Cl I2 N4 Ni
• Calculated formula: C23 H25 Cl I2 N4 Ni
• Title of publication: Heteroleptic nickel(II)-diNHC complexes and unusual ‘reverse’ carbene-transfer to silver(I)
• Authors of publication: Huynh, Han Vinh; Koh, Christine Hui Min; Nguyen, Van Ha
• Journal of publication: Dalton Trans.
• Year of publication: 2017
• a: 8.6988 ± 0.0013 Å
• b: 12.4353 ± 0.0019 Å
• c: 13.505 ± 0.002 Å
• α: 105.18 ± 0.002°
• β: 102.756 ± 0.002°
• γ: 108.548 ± 0.002°
• Cell volume: 1260.7 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0833
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1415
• Weighted residual factors for all reflections included in the refinement: 0.1537
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No