Information card for entry 7044885

Structure parameters

• Formula: C14 H39 B Cl N4 P Zn
• Calculated formula: C14 H39 B Cl N4 P Zn
• SMILES: [Zn]1(Cl)([P]([BH3])(N(CC)CC)N(CC)CC)[N](CC[N]1(C)C)(C)C
• Title of publication: Synthesis, spectroscopic characterisation and transmetalation of lithium and potassium diaminophosphanide-boranes.
• Authors of publication: Blum, M.; Kappler, J.; Schlindwein, S. H.; Nieger, M.; Gudat, D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 47
• Journal issue: 1
• Pages of publication: 112 - 119
• a: 7.7586 ± 0.0008 Å
• b: 29.766 ± 0.003 Å
• c: 9.2778 ± 0.0008 Å
• α: 90°
• β: 96.393 ± 0.004°
• γ: 90°
• Cell volume: 2129.3 ± 0.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0778
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0813
• Weighted residual factors for all reflections included in the refinement: 0.0913
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No