Information card for entry 7044886

Structure parameters

• Formula: C39 H69 B Cu N4 O P
• Calculated formula: C39 H69 B Cu N4 O P
• Title of publication: Synthesis, spectroscopic characterisation and transmetalation of lithium and potassium diaminophosphanide-boranes.
• Authors of publication: Blum, M.; Kappler, J.; Schlindwein, S. H.; Nieger, M.; Gudat, D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2017
• Journal volume: 47
• Journal issue: 1
• Pages of publication: 112 - 119
• a: 12.4854 ± 0.0009 Å
• b: 16.7096 ± 0.0012 Å
• c: 20.7813 ± 0.0017 Å
• α: 90°
• β: 90.058 ± 0.007°
• γ: 90°
• Cell volume: 4335.5 ± 0.6 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.0877
• Weighted residual factors for all reflections included in the refinement: 0.1014
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No