Information card for entry 7045693

Structure parameters

• Formula: C31 H31 Cl N3 O2 Rh
• Calculated formula: C31 H31 Cl N3 O2 Rh
• Title of publication: N-Heterotricyclic cationic carbene ligands. Synthesis, reactivity and coordination chemistry.
• Authors of publication: Iglesias-Sigüenza, Javier; Izquierdo, Cristina; Díez, Elena; Fernández, Rosario; Lassaletta, José M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 15
• Pages of publication: 5196 - 5206
• a: 7.2839 ± 0.0007 Å
• b: 13.2903 ± 0.0012 Å
• c: 14.883 ± 0.0013 Å
• α: 71.074 ± 0.003°
• β: 80.495 ± 0.003°
• γ: 79.623 ± 0.003°
• Cell volume: 1331.7 ± 0.2 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0666
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.145
• Weighted residual factors for all reflections included in the refinement: 0.156
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No