Information card for entry 7045694

Structure parameters

• Formula: C30 H34 Cl F3 N3 O3 Rh S
• Calculated formula: C30 H34 Cl F3 N3 O3 Rh S
• Title of publication: N-Heterotricyclic cationic carbene ligands. Synthesis, reactivity and coordination chemistry.
• Authors of publication: Iglesias-Sigüenza, Javier; Izquierdo, Cristina; Díez, Elena; Fernández, Rosario; Lassaletta, José M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 15
• Pages of publication: 5196 - 5206
• a: 32.9652 ± 0.0017 Å
• b: 7.9318 ± 0.0005 Å
• c: 22.4318 ± 0.0013 Å
• α: 90°
• β: 92.265 ± 0.002°
• γ: 90°
• Cell volume: 5860.7 ± 0.6 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.1093
• Weighted residual factors for all reflections included in the refinement: 0.1192
• Goodness-of-fit parameter for all reflections included in the refinement: 0.885
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No